Client Challenge
The Swiss institute faced critical limitations with conventional alumina and graphite saggers in their ultra-high-purity ceramic sintering processes (1700°C+):
- Contamination Risks: Alumina saggers leached alkaline ions into ceramic powders, compromising material purity for aerospace components.
- Thermal Shock Failures: Graphite saggers cracked after 50 thermal cycles, causing sample loss in expensive R&D experiments.
- Process Inefficiency: Frequent replacements and cleaning cycles delayed project timelines by 30%.
Core Pain Points:
- Inability to maintain material purity in high-value R&D.
- Short service life in extreme thermal cycling environments.
- High costs from failed experiments and downtime.
Kegu Solution
Kegu developed pressureless-sintered silicon carbide (SiC) saggers tailored for ultra-clean, high-temperature applications:
Technical Innovations
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Purity-Optimized Design
- Material Composition: 99.9% pure SiC (metal impurity content <50 ppm), certified by Swiss Centre for Electronics and Microtechnology (CSEM).
- Surface Finish: Polished to Ra ≤ 0.5μm to minimize powder adhesion and ensure easy cleaning.
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Extreme Environment Performance
- Temperature Range: Stable from room temperature to 1800°C, withstanding 1000+ thermal cycles (-20°C to 1800°C) without cracking.
- Corrosion Resistance: Unaffected by aggressive fluxes (e.g., Na2CO3, K2O) used in ceramic synthesis.
- Thermal Conductivity: 140 W/m·K, enabling uniform heating and reducing sintering time by 20%.
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Traceability & Quality Control
- Raw Material Purity: SiC powder sourced from ultra-clean quartz deposits (ISO 14001-certified mining).
- Production Process: Vacuum sintering at 2200°C for 20 hours under argon atmosphere to eliminate oxygen-induced defects.
- Testing Protocol:
- XRF analysis for elemental purity (conducted by SGS Switzerland).
- Dyne test for surface energy compatibility with ceramic slurries.
R&D Collaboration
- Custom Prototyping: Co-developed 50mm³ mini-saggers for micro-scale sintering experiments.
- Data Sharing: Provided real-time thermal imaging data during client’s sintering trials.
- Training Support: Hosted a technical workshop on SiC sagger maintenance for the client’s research team.
Outcome
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Purity & Process Improvements
- Contamination Eliminated: Alkaline ion leaching reduced from 1000ppm to <50ppm, meeting aerospace material standards (e.g., ASTM F2924).
- Sintering Efficiency: Cycle time reduced from 48 hours to 38 hours, accelerating R&D throughput.
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Cost & Reliability Gains
- Service Life Extended to 1000+ Cycles: 20x longer than graphite saggers, cutting replacement costs by 95%.
- Experimental Failure Rate Dropped by 85%: Consistent performance in thermal cycling eliminated sample loss.
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Market Impact
- The client’s new ceramic composites (developed using Kegu saggers) won the 2024 Swiss Technology Award for aerospace innovation.
- Kegu was listed as a preferred supplier in the client’s public procurement database for high-purity materials.
Key Data Comparison
Parameter | Kegu SiC Saggers | Traditional Alumina Saggers | Graphite Saggers |
---|---|---|---|
Max Service Temperature | 1800°C | 1600°C | 1500°C |
Thermal Cycles (until failure) | 1000+ cycles | 50 cycles | 50 cycles |
Alkaline Ion Leaching | <50 ppm | 1000+ ppm | N/A |
Sintering Time Reduction | 20% | Baseline
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